Rotating Sample Holder

1.Name: Rotating sample holder. 2.Application: Diffractometer accessories. 3.Function: Ensures good reproducibility of diffraction strength and eliminates preferred orientation.
  • Tongda
  • Liaoning, China
  • 1—2 months
  • 100 units per year

Rotating Sample Holder

In X-ray diffraction (XRD) analysis for fields such as materials science, geological analysis, and pharmaceutical R&D, the crystal orientation and grain uniformity of a sample directly impact the accuracy and reproducibility of data. Dandong Tongda Technology Co., Ltd. has designed a High-Precision Rotation Sample Stage specifically for X-ray diffractometers. Utilizing unique in-plane rotation technology, it effectively addresses measurement errors caused by coarse grains, texture, or crystal habit in samples, helping users obtain more authentic and reliable diffraction results.

Core Technical Principle: In-Plane Rotation, Precision Statistics

The core function of this sample stage is to drive the sample to rotate continuously and steadily within its own plane.

Elimination of Coarse Grain Errors: When a sample contains a small number of coarse grains, static testing can result in non-statistically representative "spotty" diffraction patterns. By continuously rotating the sample under the X-ray beam, the rotation stage ensures the beam irradiates a larger number of grains with different orientations. This homogenizes the diffraction signal, transforming discrete spots into smooth, continuous diffraction rings and significantly reducing intensity errors caused by coarse grains.

Disruption of Preferred Orientation (Texture): For samples that have developed texture (i.e., preferred orientation of grains) during processing or growth, or samples with specific crystal habits, rotational testing ensures all possible crystal planes have an equal opportunity to diffract. This breaks the dominance of fixed orientation on diffraction intensity, yielding intensity data that truly reflects the phase composition and guarantees excellent reproducibility of measurement results.

Key Performance Parameters & Functions

Rotation Mode: β-axis (sample own plane) rotation.

Rotation Speed: Adjustable from 1 ~ 60 RPM (revolutions per minute), meeting the needs of different testing scenarios.

Operation Modes: Supports constant-speed continuous rotation for routine scans, and stepping mode for more precise measurements.

High-Precision Control: Features a minimum step width of 0.1°, ensuring precise rotational positioning.

Wide Range of Application Scenarios

This rotation sample stage is an ideal choice for the following applications:

Sample preparation and pre-treatment for texture analysis of metallic materials.

Analysis of bulk or powder samples suffering from coarse grain issues.

Analysis of samples with strong preferred orientation, such as rolled plates, coatings, and platy crystals.

Quantitative phase analysis requiring extremely high reproducibility of diffraction intensity.


XRD Sample stageSample Holder

                                                              Rotating Sample Holder(XRD Sample Stage)



Specifications of Rotating Sample Holder:

Rotation modeβ axis (sample plane)
Rotation speed 1~60RPM
Minimum step width0.1°
Operating modeConstant speed rotation for sample scanning (step continuous)

Rotating Sample Holder         XRD Sample stage

                                                        Rotating Sample Holder(XRD Sample Stage)

Dandong Tongda Technology Co., Ltd. is committed to providing high-performance X-ray analysis instruments and accessories for scientific research and industrial testing. This rotation sample stage exemplifies the company's strong capabilities in precision mechanical design and deep understanding of experimental needs.

For more detailed product information, pricing, and after-sales support, please feel free to contact us directly.

https://www.tongdaxrd.com/



  • Are you a manufactuer or trading company?

    We are a professional manufactuer of XRD system.
  • Do you provide free samples?

    No free samples. As our XRD is not FMCG.
  • How about your delivery time?

    If the XRD need to be customized it depends. Otherwise basicly since reveiving advance payment need 7~30 days.
  • Do you have any qualifications?

    CE and ISO
  • What services can you provide?

    Technical guidance and operating of installation are free.

Related Products

    It is equipped with the use of X-ray diffractometer, is a kind of diffractometer accessories. It is widely used in electrochemical systems containingcontaining carbon, oxygen, nitrogen, sulfur, metal intercalation,etc.
    Multi-Function Sample Holder enables direct XRD analysis of irregular, bulk and micro-powder samples without destructive preparation. Ensures precise positioning with vacuum chuck and adjustable clamps. Ideal for advanced materials research, pharmaceuticals and geology.
    Thin film measuring accessory from Dandong Tongda Technology enhances performance by incorporating longer grating sheets. This design effectively filters out scattered radiation, reducing interference from substrate signals while significantly strengthening the thin film diffraction signals.
    Dandong Tongda's small-angle diffraction accessory precisely measures nano-multilayer film thickness (0°-5° range). Fully compatible with TD-series diffractometers, it offers plug-and-play convenience and 0.0001° reproducibility, empowering research in new energy and semiconductors.
    1. Name: Fiber accessories 2. Function: Determine the special crystal structure of the fiber, and determine the orientation of the sample according to the fiber crystallinity and half-peak width.
    1.Name: Graphite curved crystal monochromator. 2.Application: Diffractometer accessories. 3.Function: increase the peak back ratio and weak peak resolution, reduce the diffraction Angle.
    1.Name: High temperature accessories. 2.Application: Diffractometer accessories. 3.Function: Understand the changes in the crystal structure of the sample or the mutual dissolution of various substances in the process of high temperature heating.
    1. Graphite Bent Crystal Monochromator refers to a Monochromator used to generate monochromatic light for selective excitation. 2.Graphite Bent Crystal Monochromator has better stability and stronger reliability. 3. The detection of Graphite Bent Crystal Monochromator is more accurate.
    Polarographic testing using transmission or reflection Stress testing can be performed using the tilt method or the same tilt method. Thin film testing (in-plane rotation of the sample)
    thin film attachment enables precise XRD analysis of nanometer/micrometer films, ideal for semiconductors, coatings and polymers. It enhances signal, reduces substrate interference and supports high-speed scanning, widely used in R&D and quality control with TD series diffractometers.

Get the latest price? We will reply as soon as possible (within 12 hours)

top