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Fiber Accessories utilize the X-ray diffraction (transmission) method to analyze the unique crystal structure of fibers. Parameters such as crystallinity and full width at half maximum (FWHM) are used to determine the orientation degree of the sample. Main Functions and Features of Fiber Accessories: Maintaining Fiber Orientation: This is the most critical aspect. Fibers typically exhibit high anisotropy, with crystals preferentially aligned along the fiber axis. Fiber Accessories can straighten and secure fiber bundles, preserving their original orientation to measure orientation degree and distribution. Adapting to Different Sample Forms: Single Fiber: Extremely thin, requiring special clamps or frames for fixation. Fiber Bundle: Multiple fibers arranged in parallel; Fiber Accessories must align and tension them uniformly. Fiber Fabric: Materials like cloth require a flat frame to stretch them taut. Enabling Special Testing Modes: Transmission Mode: Suitable for thin fiber bundles or single fibers. Fiber Accessories include a dedicated frame to tension the fiber, allowing X-rays to penetrate the sample directly. Reflection Mode: Used for thicker fiber bundles or fabrics. Fiber Accessories provide a flat sample surface for this mode. Fiber Sample Holder: This is a simple metal or plastic frame equipped with slots or knobs. During operation, both ends of the fiber bundle are fixed to the holder, and knobs are rotated to tension the fiber, keeping it straight and parallel. The entire holder can be placed in the XRD goniometer for testing, similar to a standard sample. In summary, Fiber Accessories for XRD are specialized sample fixation devices designed for testing fibrous samples with anisotropic structures. Their core function is to maintain and regulate fiber orientation, while advanced versions may support in-situ stretching and other functionalities, providing critical insights into the orientation of crystal structures in fibers.
Originally battery accessories are experimental devices designed specifically for electrochemical testing, mainly used for in-situ characterization of battery materials during charging and discharging processes, commonly found in X-ray diffraction (XRD). 1. Core functions and application scenarios of originally battery accessories (1)Originally testing: Real time monitoring of material phase structure changes (such as crystal structure and phase transition) during battery charging and discharging can avoid sample contamination or state changes caused by battery disassembly. Support multiple electrochemical systems, including composites containing carbon, oxygen, nitrogen, sulfur, metal embedment, etc. (2) Multimodal compatibility: X-ray diffraction (XRD): used to analyze the structural evolution of positive/negative electrode materials during charge and discharge processes. 2. Structural composition and technical characteristics of originally battery accessories (1) Key components: Lower insulation cover: usually made of alumina ceramic or polytetrafluoroethylene material, containing coolant flow channels or resistance wire installation pipelines, used for temperature control. Upper conductive cover: connected to the lower insulating cover by bolts to form a closed space, with a beryllium window (diameter 15mm, thickness 0.1mm) at the top to transmit X-rays. Electrode system: originally battery accessories includes a lower electrode (with a support column) and a butterfly spring, which are electrically connected through compression fixation, simplifying the assembly process. (2) Technological innovation: Formal design: Compared with the traditional inverted method, the formal structure does not require flipping assembly, making it easy to operate in the glove box and ensuring the flatness of the beryllium window and diaphragm. Sealing and temperature control: Integrated coolant circulation pipeline and resistance wire heating device, suitable for a temperature range of -400 ℃ to 400 ℃. 3. Technical advantages of originally battery accessories (1) Simplified operation: Reduce assembly steps, decrease operating time inside glove boxes, and improve efficiency. The butterfly spring fixes the electrode without the need for rotation and tightening, avoiding interference with the simulated structure of the battery. (2) Performance improvement: The high X-ray transmittance (>90%) of beryllium windows ensures the detection signal strength. The multifunctional sample stage supports automatic sample changing and is suitable for high-throughput testing. Overall, originally battery accessoriesare important tools for electrochemical research, as their design optimizes the assembly process of traditional battery simulation structures and enhances the reliability and applicability of originally testing.
In situ medium and low temperature accessories are experimental equipment accessory used for material analysis, mainly used for in-situ testing in low or medium low temperature environments. Combined with vacuum environment, temperature control, and special window material design, it is widely used in fields such as chemistry, materials science, and catalytic research. 1. Core functions and technical parameters of in-situ medium and low temperature accessories (1) Temperature range and control accuracy Supports a temperature range of -196 ℃ to 500 ℃ in a vacuum environment (such as liquid nitrogen refrigeration), with a temperature control accuracy of ± 0.5 ℃. Some models can cover temperatures from -150 ° C to 600 ° C, suitable for a wider range of experimental needs. (2) Refrigeration method and cooling system Using liquid nitrogen refrigeration, with a liquid nitrogen consumption of less than 4L/h, and maintaining a stable temperature through a deionized water circulation cooling system. Optional low-temperature liquid nitrogen cooling system (such as Cryostream series). (3) Window Materials and Structural Design The window material is mostly polyester film (such as TD series), and some infrared configurations use KBr or SiO2 windows. The structure includes a high-pressure resistant design (such as 133kPa) and is equipped with multiple gas inlets/outlets, suitable for in-situ reactions or atmosphere control. 2. Application fields of in-situ medium and low temperature accessories (1) Material research Used for in-situ testing of X-ray diffractometers (such as TD-3500) to study changes in crystal structure and phase transition processes at low temperatures. Support research on heterogeneous catalysis, gas-solid interactions, photochemical reactions, etc. (2) Electrochemical and Battery Research It can be extended to in-situ battery accessories to test composites in electrochemical systems (such as carbon, oxygen, nitrogen, sulfur, etc.), with a temperature resistance of up to 400 ℃. (3) Industry Applications The products of Dandong Tongda Technology (TD series) have been applied in the fields of chemistry, chemical engineering, geology, metallurgy, etc., and exported to countries such as the United States and Azerbaijan. 3. Typical products and brands of in-situ medium and low temperature accessories Dandong Tongda Technology (TD Series) The accessories for X-ray diffractometers such as TD-3500 and TD-3700 emphasize high-precision temperature control (± 0.5 ℃) and efficient liquid nitrogen refrigeration. Suitable for diffuse reflectance spectroscopy measurement, providing stainless steel reaction chamber, multi window configuration (FTIR or UV Vis compatible), supporting high vacuum to 133kPa environment. Overall, in situ medium and low temperature accessories have become an important tool for material in situ analysis through precise temperature control, vacuum environment, and window design adapted to different instruments. They play an irreplaceable role in the study of low-temperature crystal structures and exploration of catalytic reaction mechanisms.
一、Core functions and application scenarios of originally battery accessories Functional positioning of originally battery accessories: 1.Implement real-time testing during battery charging and discharging processes (such as XRD, optical observation, etc.) to avoid data loss or sample contamination caused by traditional disassembly. 2.Simulate the working environment of real batteries, support temperature control, electrolyte addition, and sealing guarantee. Typical application scenarios of originally battery accessories: 1.XRD in-situ testing: Analyze the crystal phase changes of electrode materials (such as LiFePO4) during charge and discharge processes. 2.Optical in-situ observation: Observe the surface reaction of the electrode through a beryllium window (polyester film). 3.High throughput screening: supports battery performance research under multiple conditions (temperature, pressure, electrolyte). 4.Widely used in electrochemical systems containing carbon, oxygen, nitrogen sulfur, metal embedded complexes, etc. 二、Structural composition and material properties of originally battery accessories 1.Core components of originally battery accessories: Lower insulation cover: mostly made of alumina ceramic or polytetrafluoroethylene material, including installation chamber and coolant flow channel, supporting temperature control. Upper conductive cover: designed with through holes, bolted to the lower insulating cover to form a current path. Lower electrode: including top plate and support column, fixed by butterfly spring compression, simplifying the assembly process. Beryllium window (polyester film): diameter 15mm (customizable), thickness 0.1mm (customizable), used for X-ray penetration or optical observation. 2.Technical improvement of originally battery accessories: Formal assembly: replaces traditional inverted methods, simplifies the operation process, and reduces the impact of compression on the separator and positive electrode materials. Cooling and Heating: The lower insulation cover integrates a coolant channel or resistance wire pipeline, supporting temperature control of -400℃. Sealing design: The butterfly spring compresses and fixes the lower electrode, and cooperates with the installation seat airflow to blow and prevent frost and ice formation. 三、Technical advantages of originally battery accessories 1. Convenient operation of originally battery accessories: The formal structure reduces the operating time inside the glove box and lowers the assembly complexity. Modular design of components (such as replaceable beryllium windows and insulation sleeves) improves maintenance efficiency. 2. Performance parameters: Test range: Temperature range of 0.5-160℃, temperature resistance up to 400 ℃. Sealing: Supports long-term stable storage of electrolyte to avoid leakage. Compatibility: Suitable for X-ray diffractometers and other equipment.
XRD and FTIR fiber accessories provide complete material characterization solutions. XRD units analyze crystal structure and orientation, while FTIR systems identify composition through micro-imaging and ATR technology. Accessories include small-angle diffraction, parallel beam thin-film, and in-situ temperature stages for nanoscale analysis. Automated sample handling enhances efficiency. Applications span material research, industrial quality control, and scientific studies of polymer dichroism. These tools continue to evolve, driving innovations in fiber science and industrial applications.
In X-ray diffractometer, the multifunctional integrated measuring accessories are crucial component that greatly enhances the functionality and flexibility of the instrument. Used for the analysis of films on boards, blocks, and substrates, and can perform tests such as crystal phase detection, orientation, texture, stress, and in-plane structure of thin films. Basic overview of multifunctional integrated measuring accessories: Definition: They are general term for a series of additional devices or modules used in X-ray diffractometer to expand instrument functions, improve measurement accuracy and efficiency. Purpose: These attachments aim to enable X-ray diffractometer to meet a wider range of experimental needs and provide more comprehensive and accurate material structure information. The functional characteristics of multifunctional integrated measuring accessories: Perform polar diagram testing using transmission or reflection methods; Stress testing can be conducted using either the parallel tilt method or the same tilt method; Thin film testing (in-plane rotation of the sample). Technical characteristics of multifunctional integrated measuring accessories: High precision:They typically use advanced sensing technology and control systems to ensure high precision and repeatability of measurements. Automation: Many attachments support automated operations and can be seamlessly integrated with the X-ray diffractometer host to achieve one click measurement. Modular design: facilitates users to select and combine different accessory modules according to their actual needs. Application areas of multifunctional integrated measuring accessories: Widely used in fields such as materials science, physics, chemistry, biology, and geology; Evaluation of metal assembly structures such as rolled plates; Evaluation of ceramic orientation; Evaluation of crystal priority orientation in thin film samples; Residual stress testing of various metal and ceramic materials (evaluation of wear resistance, cutting resistance, etc.); Residual stress testing of multilayer films (evaluation of film peeling, etc.); Analysis of surface oxidation and nitride films on high-temperature superconducting materials such as thin films and metal plates; Glass Si、Analysis of multilayer films on metal substrates (magnetic thin films, metal surface hardening films, etc.); Analysis of electroplating materials such as macromolecular materials, paper, and lenses. The multifunctional integrated measuring accessories in X-ray diffractometer are the key to improving instrument performance. They not only enhance the functionality of the instrument, but also improve the accuracy and efficiency of measurement, providing researchers with more comprehensive and in-depth material analysis methods. With the continuous advancement of technology, these attachments will continue to play an important role in promoting scientific research in related fields to achieve more breakthroughs.
The Small angle diffractometer accessories are important accessories used in X-ray diffractometers. Small angle diffractometer accessories enable X-ray diffraction measurements to be taken within a very small angle range, from 0°to5°, for thickness testing of nano multilayer films. Plays an important role in fields such as materials science, physics, chemistry, and biology. Common types and characteristics: Parallel light thin film accessory: This accessory can generate parallel X-ray beams and is suitable for small angle diffraction measurements of thin film samples. It can improve the accuracy and resolution of measurements, reduce measurement errors caused by beam divergence, and better adapt to thin film samples of different thicknesses and properties. Multi functional sample stage: Equipped with small angle diffraction accessories, the multifunctional sample stage can provide various testing environments for samples, such as in-situ heating, cooling, stretching, etc. This makes it more convenient to study the structural changes of materials under different external conditions, and enables real-time observation of the structural response of materials during temperature, stress, and other changes. The Small angle diffractometer accessories play important role in multiple fields such as materials science, physics, chemistry, and biology by achieving small angle diffraction and precise measurement of nano multilayer film thickness, providing researchers with a powerful tool for in-depth exploration of material microstructures and properties.
Fiber accessories are tested for their unique crystal structure using X-ray diffraction (transmission) method. Test the orientation of the sample based on data such as fiber crystallinity and half peak width. A specialized component used for analyzing fiber materials such as textiles, polymer fibers, biological fibers, etc. It is commonly used to study the crystal structure, orientation, and molecular arrangement of fibers. Main functions of fiber accessories: 1. Fiber sample fixation: Fiber accessories are used to fix the fiber sample, ensuring its position and direction stability in the X-ray beam. 2. Fiber orientation analysis: By adjusting the position and angle of the sample, the crystal orientation and molecular arrangement of the fibers are studied. 3. Small angle X-ray scattering (SAXS): Some fiber attachments support SAXS for analyzing the nanoscale structure of fibers. Common types of fiber accessories: 1. Fiber stretching device: It can apply tension to fibers during XRD analysis to study structural changes under stress. 2. Rotating sample stage: allows fiber samples to rotate, facilitating the collection of diffraction data from different angles. 3. Temperature control accessories: used to analyze fiber materials at specific temperatures and study the effect of temperature on structure. Application fields of fiber accessories: 1. Materials Science: Study the crystal structure and mechanical properties of synthetic fibers such as nylon and polyester. 2. Biomaterials: Analyze the structure of natural fibers such as collagen and cellulose. 3. Textiles: Evaluate the orientation and crystallinity of textile fibers. Steps for using fiber accessories: 1. Sample preparation: Fix the fiber sample onto the attachment. 2. Adjust parameters: Set the X-ray source, detector, and sample positions. 3. Data collection: Collect diffraction patterns. 4. Data analysis: Use software to analyze diffraction data and obtain structural information. Matters needing attention: -Sample alignment: Ensure that the sample is accurately aligned with the X-ray beam. -Parameter optimization: Optimize X-ray energy, exposure time, etc. based on sample characteristics. -Data quality: Ensure clear diffraction patterns and avoid noise interference. Our company provides on-site training on instrument usage and related industry knowledge, as well as subsequent analysis software usage and maintenance, and complete machine maintenance services.
Fiber accessories are tested for their unique crystal structure using X-ray diffraction (transmission) method. Test the orientation of the sample based on data such as fiber texture and half peak width.
Originally Battery Accessory is a device used for electrochemical system research, belonging to X-ray diffractometer accessories,which allows real-time and dynamic monitoring and analysis of the battery under specific conditions. Widely used in electrochemical systems containing carbon, oxygen, nitrogen sulfur, metal embedded complexes, etc.
Fiber accessories are tested for their unique crystal structure using X-ray diffraction (transmission) method. Test the orientation of the sample based on the fiber crystallinity and half peak width of the fibers. This type of accessory is usually installed on a wide-angle diffractometer and is mainly used to study the texture of thin films on the substrate, perform crystal phase detection, orientation, stress testing, and other tests.
The graphite curved crystal monochromator is installed in front of the X-ray detector, which monochromatizes the X-rays passing through the receiving slit and only detects the K α characteristic X-ray diffractometer accessories of the X-ray spectrum. By using this device, continuous X-rays, K β characteristic X-rays, and fluorescent X-rays can be completely eliminated, enabling high signal-to-noise ratio X-ray diffraction analysis. When copper target X-ray tubes are used in conjunction with corresponding monochromators, fluorescent X-rays generated from Mn, Fe, Co, Ni based samples can be eliminated, making them suitable for analysis of various samples.