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X-ray absorption fine structure XAFS

XAFS Spectrometer achieves synchrotron-level data quality with >4M photons/s/eV flux, <0.1% stability, and a 1% detection limit. It empowers research across energy, catalysis, and materials science.

  • Tongda
  • Liaoning, China
  • 1—2 months
  • 100 units per year
  • Information

ParameterDescription
Comprehensive PerformanceEnergy Range4.5-25keV
Spectrum Acquisition ModeTransmission Mode
Photon Flux at the Sample>4×10⁶ photons/(s·eV)
Energy ResolutionXANES:0.5-1.5eV  EXAFS:1.5-10eV
 X-ray PathHelium purge path to minimize air absorption
RepeatabilityReproducible energy drift < 50 meV
StructureThe dual Rowland circle configuration eliminates the need
for light source switching during XAFS measurements.
Utilizing a single dedicated XAFS X-ray source to generate a dual X-ray beam,
the system provides two energetically monochromatic X-rays
through dual Rowland circles and dual monochromators.
This enables simultaneous characterization of two metal elements
within the same sample, permitting parallel analysis
 of the local atomic structures of both metallic elements.
X-ray SourcePower2.0 kW; High voltage: 10-40 kV; Current: 1-50 mA
TargetStandard with W/Mo targets; other target materials available as options
MonochromatorTypeSpherical analyzer crystal with 500 mm radius of curvature and 102 mm size
DetectorTypeLarge-area SDD with a 150 mm² active area
 Additional Configurations Sample Changer18-position sample changer for continuous automated testing of multiple samples
 In Situ Sample CellIn situ cells for various conditions: electrocatalysis,
temperature-varying, multiphysics fields, and mechanical testing
Analyzer CrystalSpecialized crystal monochromator for specific-element analysis


Core Advantages:

Highest Photon Flux: Our product delivers a photon flux exceeding 4,000,000 photons/s/eV, offering spectrum acquisition efficiency several times higher than comparable systems. This enables data quality on par with synchrotron radiation sources.

Exceptional Stability: The instrument features excellent monochromatic light intensity stability, with variations of less than 0.1%. Reproducible energy drift during repeated acquisitions is maintained below 50 meV.

1% Detection Limit: The combination of high flux, superior optical path optimization, and exceptional source stability ensures the acquisition of high-quality EXAFS data, even for elemental concentrations as low as 1%.

Instrument Principle:

The X-ray Absorption Fine Structure (XAFS) spectrometer is a powerful tool for investigating the local atomic and electronic structure of materials. It is widely applied across various prominent fields, including catalysis, energy research, and nanoscience.

X-ray absorption fine structure

Laboratory Monochromator XES Testing Geometry

XAFS


Laboratory Monochromator XAFS Testing Geometry

X-ray absorption fine structure


Manganese (Mn) Data and Mn K-edge XAFS Data: Consistent with Synchrotron Radiation Source Quality

XAFS


Kβ Emission Spectrum Data of Iron (Fe) Sample: Core-to-Core XES and Valence-to-Core XES

Test Data

Foil EXAFS Data

X-ray absorption fine structure


Applications

This XAFS spectrometer finds wide-ranging applications, empowering clients to make breakthroughs across multiple fields:

New Energy: Used in the study of fuel cells, hydrogen storage materials, lithium-ion batteries, etc. It can analyze the dynamic changes in the valence state and coordination environment of central atoms during catalytic processes.

Industrial Catalysis: Applicable to research areas like nanoparticle catalysis and single-atom catalysis. It can characterize the morphology of catalysts on supports and their interactions with the support material.

Materials Science: Employed for the characterization of various materials, the study of complex systems and disordered structures, as well as investigating the properties of surface and interface materials.

Environmental Science: Can be utilized to analyze heavy metal contamination in samples such as soil and water, determining the valence state and concentration of elements.

Biomacromolecules: Can be used to study the local atomic structure around metal centers in metallobiomolecules .

XAFS




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